Sediment Texture Analysis · 417 Samples · 12 Stations · 2016–2024

Grain Size Does Not Control Contamination

Conventional sediment chemistry predicts that finer-textured sediments carry more metal contamination than coarser ones, due to greater surface area and cation-exchange capacity. In the Pilcomayo's Potosí headwaters, mining-derived loading saturates all texture classes — the bulk grain-size signal is overridden, even though specific seasonal × texture interactions remain measurable and matter for sampling design and remediation targeting.

417 Potosí Samples 5 USDA Texture Classes 12 Stations 2016–2024
Orientation

What "Texture" Means and Why It Usually Matters

In typical fluvial systems, sediment texture predicts metal accumulation: finer-textured sediments — loam, silty loam — accumulate significantly more metal than coarser ones — sand, sandy loam — because they offer greater surface area and higher cation-exchange capacity per gram. The five USDA texture classesThe U.S. Department of Agriculture's soil/sediment classification by relative proportions of sand, silt, and clay. Five classes appear in this study: sand, sandy loam, sandy clay loam, loam, and silty loam. used in this analysis (sand, sandy loam, sandy clay loam, loam, silty loam) span that coarse-to-fine continuum. The Pilcomayo dataset was built to test whether this textbook relationship holds in a basin dominated by an upstream point-source.

Expected — typical fluvial system ↑ more metal Observed — Pilcomayo (As 15.0–20.7 mg/kg) ≈ flat Sand Sandy Loam Sandy Clay Loam Loam Silty Loam coarse fine →

Five USDA texture classes ordered coarse to fine. Top line: the gradient a textbook fluvial system would produce. Bottom line: what the Pilcomayo actually shows — arsenic medians 15.0–20.7 mg/kg across all five classes. The flat line is the finding.

The Core Result

Source Dominance Overrides Texture — Through Sorption-Site Saturation

Across 417 Potosí sediment samples spanning the five USDA texture classes — sand, sandy loam, sandy clay loam, loam, and silty loam — arsenic medians remain in the narrow range 15.0 to 20.7 mg/kg regardless of class. The bulk texture-contamination relationship that holds in textbook fluvial systems is not detectable here. The mechanism is not noise: mining-derived loading is so persistent and so concentrated that it has saturated the available sorption sitesThe process by which a dissolved metal attaches to a solid surface (sediment particle, mineral phase). A 'sorption site' is one such attachment location; once all sites are occupied, additional metal stays in solution. in every texture class simultaneously, from coarse sand to silty loam.

Null Result as Evidence — Across 417 Potosí samples in five USDA texture classes (sand, sandy loam, sandy clay loam, loam, silty loam), arsenic medians range only from 15.0 to 20.7 mg/kg. The conventional texture-contamination relationship simply does not apply when a point-source mine has been discharging into the headwaters for centuries. The narrow range is the diagnostic — it indicates sorption-site saturation, not the absence of a mechanism.
Theory meets data: the same saturation mechanism appears in the partitioning analysis. The partitioning page documents a strongly negative clay-Cd correlation (ρ = −0.404, p < 0.0001, n = 255) and interprets it as sorption-site saturation in clay-rich downstream sediments — metals from upstream mining have already occupied the available exchange sites. That is the same mechanism operating here at the texture-class scale: when source loading is sufficient to saturate every available site, finer textures stop carrying more metal than coarser ones. The bulk null on this page and the negative clay-Cd correlation on the partitioning page are two views of one process.
The Implication for Remediation — Strategies that target fine-grained sediments specifically (e.g., dredging clay-rich deposits, capping silty loam reaches) will miss a large fraction of the total metal inventory in the Potosí zone. Sand and sandy loam — the modal classes in the headwaters — carry contamination at the same order of magnitude as the finer classes. Metal removal must target the high-concentration source-proximal corridor, not grain-size classes.
Metal concentration by texture class at Potosí stations

What you are looking at: each panel shows one metal. The horizontal axis is texture class, ordered coarse (sand) to fine (silty loam). Box heights are concentration distributions; flat box heights across the row mean texture does not predict concentration. Detail: arsenic, lead, cadmium, and mercury medians across the five USDA texture classes at all 12 Potosí stations (n = 417). Arsenic medians stay in the 15.0–20.7 mg/kg band, the diagnostic narrow range that anchors the saturation finding. Units: mg/kg dry weight.

Station-level dot plots: concentration vs. grain size

What you are looking at: each dot is one sediment sample, plotted at its measured concentration (vertical) against its texture class (horizontal). If finer textures carried more metal, the dot cloud would tilt upward to the right. It does not. Detail: individual-sample concentrations vs. USDA texture class for all four priority metals across the 12 Potosí stations. The absence of any rising trend confirms the bulk null: at the sample scale as at the class scale, source proximity — not grain size — sets the concentration.

Spatial Gradient

Station-Level Summary — A 35× Source-to-Distal Drop

Station-level medians make the spatial gradient visible. San Antonio–Potosí, the most source-proximal station, has a median sediment arsenic of 284 mg/kg; Misión La Paz at the Argentina/Paraguay border records a median of 8 mg/kg — a 35× drop along the same monitoring transect. That spatial gradient dwarfs any within-station variation across texture classes, and is the empirical reason source dominance overrides texture at the bulk level.

Station Region Samples As median (mg/kg) Pb median (mg/kg) Cd median (mg/kg) Hg median (mg/kg)
San Antonio–Potosí Potosí Mining Zone 58 284 296 1.8 0.4
Tarapaya Potosí Mining Zone 42 187 241 1.4 0.2
Naciente Potosí Mining Zone 38 124 156 0.9 0.1
Camblaya Bolivia non-Mining 31 42 58 0.4 0.03
Villa Montes Bolivia non-Mining 35 22 31 0.2 0.02
Pozo Hondo Bolivia non-Mining 29 11 14 0.1 <0.01
Misión La Paz Argentina/Paraguay 24 8 9 0.08 <0.01
Why this matters for the texture story. The 35× gradient between San Antonio–Potosí (As 284 mg/kg) and Misión La Paz (As 8 mg/kg) is more than an order of magnitude larger than any texture-driven variability within a single station. The station you sample matters far more than the texture class — sample design that varies texture without varying station will return a flat result; sample design that varies station will return the basin's real signal.
Station concentration profiles

What you are looking at: each row is one Potosí station, ordered by descending arsenic median. Bar heights show median concentrations. The descent from top to bottom is the 35× source-to-distal gradient. Because the bars are station-level medians (not texture-resolved), the figure shows what dominates: the spatial decay, not within-station texture variation. Detail: all 12 monitoring stations, As/Pb/Cd/Hg medians, units mg/kg dry weight. Stations are ordered by As median to visualize the spatial decay from source-proximal to distal.

Where the Null Breaks

Seasonal × Texture Interactions

The bulk relationship is overridden — but specific season × texture combinations are not. When dry-season hydrology is layered onto the texture data, two large enrichments emerge: cadmium concentrations in sandy loam rise 157% from the wet to the dry season, and arsenic concentrations in silty loam rise 531% over the same hand-off. These are the texture-dimension fingerprint of the same seasonal water↔sediment cycle described on the spatiotemporal page, and they are operationally important: dry-season sampling in finer classes captures peak concentrations that wet-season sampling misses.

Cd · Sandy Loam · Dry Season
+157%
wet → dry season
As · Silty Loam · Dry Season
+531%
wet → dry; n = 14, interpret with caution
As · Sand · Reference
Stable
bulk null holds in coarse classes
Two findings, one cycle. The dry season concentrates metals in sediment because reduced stream discharge lowers dilution of mining effluent — the inverse of the water-phase pulse the spatiotemporal page describes. The 157% Cd-in-sandy-loam and 531% As-in-silty-loam enrichments are the same cycle resolved into texture classes: certain classes act as the seasonal accumulation reservoirs. The 531% silty-loam As result is based on n = 14 dry-season observations and should be interpreted with caution, but the direction and magnitude are consistent with the broader cycle.
Sampling-design implication. Studies that average over wet and dry seasons, or that focus on coarser classes, will miss these enrichments and conclude — incorrectly — that texture is irrelevant. To detect the texture × season signal, dry-season campaigns must include sandy loam and silty loam samples specifically, and report the n in each cell. The bulk null is real; so are the cell-level enrichments — both are the report's findings, not contradictions.
Seasonal texture and concentration patterns by texture class

What you are looking at: wet- and dry-season median concentrations by texture class, side by side. The cells that matter most are sandy loam (Cd) and silty loam (As) — those are where the dry-season bar towers over the wet-season bar. Detail: per-metal seasonal medians by USDA texture class at Potosí stations. The 157% sandy-loam Cd enrichment (wet → dry) and the 531% silty-loam As enrichment (wet → dry, n = 14, interpret with caution) are quantified directly here. Units: mg/kg dry weight. Wet season = November–April; dry season = May–October.

Confounder for Temporal Trends

Textural Composition Has Shifted Over Time

The eight-year monitoring record reveals a compositional shift in the basin's sediment texture itself. Sand was the modal class in early campaigns from 2016 to 2018; from 2019 onward, sandy loam took over as the dominant class. The drivers are not fully resolved — the shift may reflect changes in sampling coverage, interannual hydrological variability affecting sediment transport, or a combination of both. Whatever the cause, this matters for trend interpretation: a move toward finer sediment textures in later campaigns could independently influence metal retention capacity, and any long-term concentration trend that does not control for textural composition risks confounding the two effects.

Read this before interpreting any 8-year trend. When sediment texture composition itself changes over the monitoring window, a rising or falling concentration trend can reflect (a) a change in real loading from upstream, (b) a change in the proportion of finer classes that retain more metal, or (c) both. The Pilcomayo record contains all three possibilities. Trend statements throughout this site are framed at the bulk level (texture-aggregated medians); the 2024 mercury and cadmium spikes discussed in the next section are large enough to exceed any plausible textural-shift effect, but smaller trends should be reported with this confounder acknowledged.
Basin-wide sediment textural classification distribution across 16 sampling campaigns

What you are looking at: stacked bars showing the proportional abundance of the five USDA texture classes across 16 sampling campaigns from 2016 to 2024. Each bar is one campaign; colored segments are the share of that campaign's samples in each class. The visual compositional shift around 2019 is the sand → sandy loam transition. Blue shading marks wet-season campaigns (November–April). Detail: Figure 4.4.2a from the report. Use this figure as the diagnostic before reading any of the 2016–2024 long-term trend visualizations elsewhere on the site.

Seasonal patterns by texture class across the 8-year record

What you are looking at: seasonal patterns by texture class plotted across the eight-year monitoring window. The figure resolves both axes — season and texture — into the temporal record. Cells with persistent dry-season elevation in finer classes are the long-term face of the seasonal × texture finding above. Detail: per-metal seasonal-by-texture concentrations, all 16 sampling campaigns from 2016 to 2024 at Potosí stations. Read together with the textural-distribution figure above to separate real loading change from compositional shift.

Second Act · 2024 Emerging Contamination

A Synchronous Mercury and Cadmium Spike — and What It Implies

The textural shift above is a confounder; the 2024 emerging-contamination event is not. Across all five texture classes, two metals with very different geochemical behaviors spiked together in 2024 — mercury reached its eight-year high in the wet season, and cadmium reached its eight-year high in the same year. Synchronous spikes in metals with distinct binding chemistries do not appear from gradual accumulation. They appear when something changes upstream.

Mercury trajectory: near-zero through 2019 → 1.3 mg/kg (2021 dry season) → 2.3 mg/kg (2024 wet season). The 2024 figure is more than thirteen times the USEPA freshwater sediment guideline of 0.174 mg/kg. The rise occurred over roughly five years from a near-zero baseline, not gradually across the eight-year monitoring window. Anchored to the regulatory threshold rather than the start of the record, the magnitude becomes legible: 13× exceedance, in a metal that was effectively absent five years earlier.
Cadmium synchronous spike: 5.0 mg/kg in 2024 — the highest value in the eight-year record. Cadmium had been broadly stable across the monitoring window, with no significant long-term trend across the texture classes. The 2024 value is a step-change, not a continuation. It is the synchronicity with the mercury spike — same year, same basin, geochemically unrelated metals — that turns this from two independent observations into a single signal.
0 1.0 2.0 mg/kg USEPA 0.174 Cd: 5.0 (synchronous) 1.3 2.3 2016 2017 2018 2019 2020 2021 2022 2023 2024 Hg basin-wide median (mg/kg) USEPA freshwater sediment guideline (0.174 mg/kg)

Mercury trajectory at Potosí stations, 2016–2024 (basin-wide median, mg/kg). Dashed red line: USEPA freshwater sediment guideline. The 2024 value (2.3 mg/kg) is more than thirteen times the regulatory threshold; the gold ring marks the synchronous cadmium spike (5.0 mg/kg) in the same year.

What synchronicity rules in, and what it rules out. Mercury and cadmium have distinct geochemical behaviors and distinct host phases — Hg follows organic matter and sulfide; Cd, in this basin, sits on calcium-phosphate minerals (see partitioning, Cd story). They do not normally rise together from gradual accumulation processes. Their simultaneous spike in a single year suggests a discrete upstream source change rather than gradual accumulation. Two candidate explanations are consistent with the data: (1) shifts in ore-processing methods at existing operations, or (2) the introduction of artisanal gold amalgamation activity in the headwater catchment. The data here does not distinguish between these two explanations.
Urgent source identification is required before remediation planning for these metals can proceed. Until the upstream source is identified and characterized, treatment design for Hg and Cd has no target: a sediment-stabilization approach that addresses gradual accumulation will not contain a discrete new source, and a treatment scaled to historical loading will under-perform if loading has step-changed. The 13× USEPA exceedance and the synchronous Cd spike together place this on a different timescale than the rest of the basin's contamination — recent, accelerating, and not yet attributed.
Synthesis

From Texture Data to Targeting Decisions

What the texture data prove. At the bulk level, source dominance combined with sorption-site saturation overrides texture — the same mechanism that produces the negative clay-Cd correlation on the partitioning page (ρ = −0.404). At the seasonal × texture level, finer classes show large dry-season enrichments (157% Cd in sandy loam, 531% As in silty loam with the n = 14 caveat) — the texture-dimension fingerprint of the seasonal cycle the spatiotemporal page describes. The eight-year record reveals a sediment-textural shift (sand → sandy loam from 2019) that must be controlled for in temporal-trend analyses. And in 2024, mercury and cadmium spiked synchronously to record highs — Hg to 13× the USEPA freshwater sediment guideline — pointing to a discrete new upstream source.

What it implies for action. Remediation must target the source-proximal corridor over individual texture classes — sand and sandy loam carry as much metal as silty loam in the headwaters, and the 35× station gradient swamps any within-station texture variation. Dry-season campaigns must include sandy loam and silty loam samples to detect peak concentrations the bulk null hides. Eight-year trend statements should control for the 2019 textural shift before being interpreted as real loading change. And the 2024 mercury and cadmium spikes are large enough to step around all of the above — they point at a source that has not been identified, and treatment design cannot proceed without that identification.

Continue Reading